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ISHS Acta Horticulturae 677: III WOCMAP Congress on Medicinal and Aromatic Plants - Volume 3: Perspectives in Natural Product Chemistry

IDENTIFICATION OF VOLATILE CONSTITUENTS IN ARTABOTRYS HEXAPETALUS FLOWERS USING SIMPLE HEADSPACE SOLVENT-TRAPPING TECHNIQUE IN COMBINATION WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY AND RETENTION INDICES

Authors:   C. Mahidol, N. Chimnoi, D. Chokchaichamnankit, S. Techasakul
Keywords:   esters, odor, solid-phase microextraction, hydrodistillation, solvent extraction
Abstract:
The compositions of the volatiles from Artabotrys hexapetalus flowers were investigated. These volatiles were obtained by simple headspace-solvent trapping technique with dichloromethane as the trapping solvent. The investigation was performed in combination of gas chromatography-mass spectrometry (EI and PCI) and retention indices. Seventeen components were identified with ethyl acetate (47.3%), ethyl isobutanoate (9.2%), isobutyl acetate (26.8%) and ethyl butanoate (9.7%) as the major components. The extract was also compared with those obtained by solid-phase microextraction (SPME), solvent extraction and hydrodistillation. The odor of the solution from this technique was similar to that of the fresh flowers and differed from that obtained by solvent extraction and hydrodistillation.

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